Tetra­iodido[methyl­enebis(diphenyl­phosphine oxide)-κ2 O:O′]tin(IV) chloro­form solvate

نویسندگان

  • Allison M. Caldwell
  • Joseph M. Tanski
چکیده

The title compound, [SnI(4)(C(25)H(22)O(2)P(2))]·CHCl(3), crystallized from a chloro-form solution of SnI(4) and the diphosphine CH(2)(PPh(2))(2) exposed to air. The monomeric complex displays a distorted octa-hedral coordinaton for the tin(IV) atom with average Sn-I and Sn-O bond lengths of 2.79 (2) and 2.15 (1) Å, respectively.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Tetra­chloridodi-μ3-oxido-tetra­kis­(μ2-propan-2-olato-κ2 O:O)ditin(II)ditin(IV)

The centrosymmetric tetranuclear title molecule, [Sn4(C3H7O)4Cl4O2], contains two types of Sn atoms, Sn(II) and Sn(IV). The Sn(II) atom has a trigonal-pyramidal coordination environment and is bonded to two O atoms from two iso-propano-late groups and one μ3-oxide atom. The Sn(IV) atom has an octa-hedral coordination environment, formed by two chloride atoms, two μ3-oxide atoms and two O atoms ...

متن کامل

[μ-1,4-Bis(diphenyl­phosphino­yl)butane-κ2 O:O′]bis­[cyclo­pentyl­diphen­yl(trifluoro­acetato-κO)tin(IV)]

The mol-ecule of the dinuclear title compound, [Sn(2)(C(5)H(9))(2)(C(6)H(5))(4)(C(2)F(3)O(2))(2)(C(28)H(28)O(2)P(2))], lies on a center of inversion at the mid-point of the central C-C bond of the bridging phosphine oxide ligand. The Sn atom is five-coordinate in a trans-C(3)SnO(2) trigonal-bipyramidal geometry.

متن کامل

catena-Poly[[cyclo­hexyl­diphenyl­tin(IV)]-μ-hydroxido-κ2 O:O]

The title polymeric mixed-organyl tin hydroxide, [Sn(C(6)H(5))(2)(C(6)H(11))(OH)](n), hass a hydroxide-bridged chain structure; the tin center shows trans-C(3)SnO(2) trigonal bipyramidal coordination. The Sn atom lies on a special position of site symmetry m; the symmetry element relates one phenyl ring to the other and also relates one half of the cyclo-hexyl ring to the other half.

متن کامل

(2,2′-Bipyridine-κ2 N,N′)bis­(N-ethyl-N-phenyl­dithio­carbamato-κ2 S,S′)cadmium(II) chloro­form solvate

In the title compound, [Cd(C(9)H(10)NS(2))(2)(C(10)H(8)N(2))]·CHCl(3), the Cd(II) atom exists in an all-cis distorted octa-hedral geometry. Chelation is isobidentate for one dithio-carbamate ligand and anisobidentate for the other. The chloroform solvent mol-ecule is disordered over two positions of equal occupancy.

متن کامل

catena-Poly[[tris­(4-fluoro­benz­yl)tin(IV)]{μ-[(N,N-diisopropylcar­bamo­thioyl)sulfanyl]acetato-κ2 O:O′}]

In the title compound, [Sn(C(7)H(6)F)(3)(C(9)H(16)NO(2)S(2))](n), the Sn atom is coordinated in a slightly distorted, trans-C(3)SnO(2) trigonal-bipyramidal environment. Symmetry-related Sn atoms are bridged by diisopropyl-dithio-carbamoylacetato ligands, forming a one-dimensional polymer along [001].

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:

دوره 64  شماره 

صفحات  -

تاریخ انتشار 2008